On-line analyte preconcentration with atomic spectrometric detection
نویسندگان
چکیده
منابع مشابه
On-line analyte preconcentration with atomic spectrometric detection
Pre-concentration of analytes, or matrix removal to overcome interferences using mini- or micro-columns of exchange media prior to atomic spectrometric detection is becoming increasingly more common. This paper is a review of some of the more recent applications of chelating, ion exchange and other resins and gels that have been used to accomplish this.
متن کاملAtomic Absorption Spectrometric Determination of Lead after Extraction and Preconcentration with 5-Br-PADAP
Lead is quantitatively retained on 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol (5-Br-PADAP)-ammonium tetraphenylborate with microcrystalline naphthalene or by a column method in the pH range 4.0-6.0 from a large volume of aqueous solutions of various samples with preconcentration factor of 60. After filtration, the solid mass consisting of the lead complex and naphthalene was dissolved wi...
متن کاملOn-line separation and preconcentration of silver ion on amidino-thiourea immobilized glass beads packing in flow injection analysis with atomic absorption spectrometric detection.
Amidino-thiourea immobilized glass beads (AGB I) were prepared and used as the microcolumn packing for the flow injection (FI) on-line separation and preconcentration of Ag(I) coupled with atomic absorption spectrometry (AAS) determination. Base metal ions and anions with a concentration of 2.0 mg mL(-1) had no interference with the determination of Ag(I). The limit of detection (LOD) of Ag(I) ...
متن کاملFlame atomic absorption spectrometric determination of chromium(VI) by on-line preconcentration system using a PTFE packed column.
A new, sensitive and robust time-based flow injection (FI) method for on-line preconcentration and determination of ultra trace amounts of chromium(VI) by flame atomic absorption spectrometry (FAAS) has been elaborated. The sample is initially mixed on-line with ammonium pyrrolidine dithiocarbamate (APDC) and the Cr(VI)-PDC chelate is absorbed quantitatively on a mini-column packed with polytet...
متن کاملatomic absorption spectrometric determination of lead after extraction and preconcentration with 5-br-padap
lead is quantitatively retained on 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol (5-br-padap)-ammonium tetraphenylborate with microcrystalline naphthalene or by a column method in the ph range 4.0-6.0 from a large volume of aqueous solutions of various samples with preconcentration factor of 60. after filtration, the solid mass consisting of the lead complex and naphthalene was dissolved with 5...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Journal of Automatic Chemistry
سال: 1991
ISSN: 0142-0453
DOI: 10.1155/s1463924691000445